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3. 1 Techniques of Comminution 35 3. 2 Solid-Solid Reactions 42 3. 2. 1 Mixing and Calcination 42 3. 2. 2 Modem Techniques 45 3. 3 Solution Techniques 46 3. 3. 1 Precipitation and Co-precipitation 46 Forced Hydrolysis 3. 3. 2 49 3. 3. 3 Hydrotbennal Synthesis 51 The Sol-Gel Process 3. 3. 4 53 3. 3. 5 Hydrolysis of Metal-Organics 56 The Emulsion Process 3. 3. 6 56 Solvent Vaporization 3. 4 59 3. 4. 1 Simple Evaporation 59 3. 4. 2 Spray Drying 60 3. 4. 3 Spray Pyrolysis 64 3. 4. 4 Freeze Drying 66 3. 5 Vapour-Phase Techniques 68 3. 5. 1 Vaporization-Condensation 68 3. 5. 2 Vapour-Vapour Reaction 68 3. 5. 3 Vapour-Liquid Reaction 70 3. 5. 4 Vapour-Solid Reaction 71 3. 6 Precursor Decomposition 72 3. 6. 1 Salt Decomposition 72 3. 6. 2 Polymer Pyrolysis 73 4. Synthetic Powders : Options in Preparation 75 4. 0 Introduction 75 4. 1 Single and Multiple Oxide Powders 75 4. 1. 1 Aluminium Oxide 75 4. 1. 2 Zirconium Oxide 85 4. 1. 3 Titanium Oxide 96 4. 1. 4 Magnesium Oxide 99 4. 1. 5 Silicon Dioxide 101 4. 1. 6 Rare Earth Oxides 105 Yttrium Oxide 105 Cerium Oxide 106 4. 1. 7 Zinc Oxide 107 [vi] 4. 1. 8 Mullite 110 4. 1. 9 Magnesium Aluminate Spinel 114 4. 1.
Ceramic powder synthesis and processing are two of the most important technologies in chemical engineering and the ceramics-related area of materials science. This book covers both the processing and the synthesis ofceramic powders in great depth and is indeed the only up-to-date, comprehensive source on the subject available.The application of modern scientific and engineering methods to the field of ceramic powder synthesis has resulted in much greater control of properties. Fundamentals of Ceramic Powder Processing and Synthesis presents examples of these modern methods as they apply to ceramic powders. The book is organized to describe the natural and synthetic raw materials that compris...
The book consists of papers on several methods used in the preparation of basic ceramic powders with the required particle size distribution and purity. Processing methods such as spray drying, thermal decomposition of organometallic complexes, the sol-gel process and solution sythesis, among others, have been discussed.
The current book contains twenty-two chapters and is divided into three sections. Section I consists of nine chapters which discuss synthesis through innovative as well as modified conventional techniques of certain advanced ceramics (e.g. target materials, high strength porous ceramics, optical and thermo-luminescent ceramics, ceramic powders and fibers) and their characterization using a combination of well known and advanced techniques. Section II is also composed of nine chapters, which are dealing with the aqueous processing of nitride ceramics, the shape and size optimization of ceramic components through design methodologies and manufacturing technologies, the sinterability and proper...
This collection emphasizes the advances of powder and ceramic/glass materials in the fundamental research, technology development, and industrial applications. Ceramic materials science covers the science and technology of creating objects from inorganic, non-metallic materials, and includes design, synthesis, and fabrication of ceramics, glasses, advanced concretes, and ceramic-metal composites. In recent years, the hybrids of ceramic and metallic materials have received plenty of interdisciplinary inspirations and achievements in material processes and functional applications including ionic conductors, catalysis, energy conversion and storage, superconductors, semiconductor, filtrations, ...
Ceramic Processing is the first comprehensive, stand alone, multi-authored book on advanced ceramic processing. It provides an overview of the important processing steps involved in the fabrication of advanced ceramics for structural and functional applications.
Special ceramics, Ceramics, Cermets, Particulate materials, Ceramic and glass technology, Testing conditions, Compaction tests, Compression testing, Test equipment, Specimen preparation, Mechanical testing, Reproducibility
This edition is dedicated to researching the effect of high-pressure explosive compaction of ceramics powder on the process of binderless sintering and the properties of resulting functional ceramic materials.