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Information requirements of measurement programmes; Sampling; Basic problems and aims of sampling; Time and frequency of sampling; Overall design of sampling programmes; Procedures for obtaining samples of waters; Preparation, transport, storage, and stability of samples; The nature and importance of errors in analytical results; Random error; Systematic error; Accuracy; Effects of errors on decision making; Need to estimate analytical errors; Estimation and control of the Bias of analytical results; Detailed consideration and assessment of individual sources of Bias; Assessment of the overall Bias of analytical results; Estimation and control of the precision of analytical results; Model of Random errors; Achievement of specified accuracy by a group of laboratories; Types of inter-laboratory studies; Reporting analytical results; Reporting results close to the lower concentration limit of an analytical system; The selection of analytical methods; General precautions in water-analysis laboratories; Analytical techniques; Automatic and on-line analysis; Computers in water analysis; The scope for computing in water analysis and related activities.
This book brings together in one place all available information on the determination of metals, organics, organometallic compounds, anions, cations, dissolved gases, radioactive substances and miscellaneous determinands in natural and treated waters.
The purpose of this book is to draw together the world-wide literature on the occurrence and analytical determination of all types of organic, organometallic and inorganic compounds in soils, animals, crops, plants, grains, dairy products and processed foods. Animal feed and fertilizers are also discussed.
This book contains contributions based on the proceedings of two symposia on food contamination held in London in April 1989 and May 1990, both of which were organised jointly by the Environment, Food Chemistry and Toxicology Groups of the Royal Society of Chemistry. The aim of these meetings was to assess the extraneous chemical contamination of food from two sources: firstly, food-chain contaminants - the presence of plant toxicants of fungal metabolites in food, or the contamination of food from environmental sources (airborne, aquatic and terrestrial); and secondly, food-production contaminants - contaminants of man-made origin brought about by a desire to facilitate food production and ...
Provides the basic skills and information required to prepare an environmental sample for analysis. Divided into two sections, i.e. Inorganic Analysis and Organic Analysis, this book covers selected techniques, principally atomic spectroscopy and chromatography. Using flow diagrams to augment the experimental information, it highlights the most appropriate methods and the likely results. Detailed experimental information provided in an easy-to-follow style with illustrations Describes the specific sample preparation approaches necessary to analyse a particular sample type Discussion of selected literature sources highlights the most appropriate methods and the likely results obtained
From the Introduction With regard to nitrate and nitrite, the perceived hazards are to the ecological balance in rivers and lakes, and to human health. Increased nitrate levels in river water lead to increased growth of algae and consequent decrease in the level of biologically available oxygen (BAO). In extreme forms, the algae form unsightly blooms on the water surface, and the BAO level falls below that necessary to support fish and other animal life. At this extreme, there is little dispute that efforts should be made to restore the ecological balance, and this is best achieved by reversing the increase in nitrate concentration that caused the problem. The health hazards are less clear, ...
Extensively revised and updated, Handbook of Water Analysis, Third Edition provides current analytical techniques for detecting various compounds in water samples. Maintaining the detailed and accessible style of the previous editions, this third edition demonstrates water sampling and preservation methods by enumerating different ways to measure c
This book provides a unique source of reference on the chemical analysis of potentially contaminated land. It assists in specifying appropriate analyses, relevant strategies for carrying out analyses, and methods of interpreting results within the new risk-based legislative framework for contaminated land. It addresses all aspects of the analysis, from delivery of the samples to the laboratory to the presentation of the results to the clients. Emphasis is placed on concentrated, tabular data, wherever possible. Problems of analysis are highlighted and solutions are proposed. Asbestos is covered in detail in the chapter on inorganic parameters, and a chapter is included on the new techniques of ecotoxicity measurement. Directed equally at the analytical chemist and the environmental scientist or engineer responsible for commissioning analyses of potentially contaminated soil or water samples, the book is written in a way that will prove helpful to both new and experienced practitioners. As such, it is one of the first volumes to bridge the gap between the customer and the supplier.
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Determination of Metals in Natural and Treated Waters draws together all the available literature and presents in a systematic fashion the latest analytical techniques for detecting metals in non-saline and saline natural and treated water. Broad outlines of different methods and their applicability in certain situations are given allowing the chemist to choose appropriate test methods. This volume is an essential reference for environmental analytical chemists, toxicologists and the medical community in the water, agrochemistry, fisheries and waste management industries and the public sector, including enforcement and public health.