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Microwave-assisted alkaline hydrolysis of PET can be 20 times faster and at lower temperatures. This work presents a novel industrial microwave applicator at 2.45 GHz with homogeneous distribution to support this reaction, which allows an efficient and continuous operation. In addition, an innovative dielectric and calorimetric measurements setup is presented. Furthermore, the modelling of the reaction kinetics based on the measured dielectric parameters is presented.
Das Institut für Hochleistungsimpuls- und Mikrowellentechnik (IHM) forscht auf den Gebieten der gepulsten Leistung und der Hochleistungsmikrowellentechnologie. Die Anwendungen für Impulsstromtechnologien reichen von der Materialbearbeitung bis zur Bioelektrik. Hochleistungsmikrowellentechnologien konzentrieren sich auf HF-Quellen (Gyrotrons) für die Elektronenzyklotronresonanzheizung von magnetisch eingeschlossenen Plasmen und auf Anwendungen für die Materialbearbeitung bei Mikrowellenfrequenzen. - The Institute for Pulsed Power and Microwave Technology (IHM) is doing research in the areas of pulsed power and high-power microwave technologies. Applications for pulsed power technologies are ranging from materials processing to bioelectrics. High power microwave technologies are focusing on RF sources (gyrotrons) for electron cyclotron resonance heating of magnetically confined plasmas and on applications for materials processing at microwave frequencies.
High energy demand is one reason for high costs of carbon fibers. One option to decrease them is to use microwave heating instead of conventional heating. In this work, steps towards a microwave assisted process during the stabilization phase are presented. In-situ dielectric measurements are performed and a reaction kinetics model is setup in connection to the dielectric loss. This allows to calculate a stabilization degree and fiber temperatures leading to a basic process understanding.
This work presents the development of a new sub-THz source for the generation of trains of coherent high-power ultra-short pulses at 263 GHz via passive mode-locking of two coupled helical gyro-TWTs. For the first time, it is shown that the operation of such passive mode-locked helical gyro-TWTs in the hard excitation regime is of particular importance to reach the optimal coherency of the generated pulses. This could be of particular interest for some new time-domain DNP-NMR methods.
Ein Gyrotron wird in magnetisch eingeschlossenen Plasmaexperimenten für Heizung, Stromtrieb, Plasmastabilisierung und Plasmadiagnostik verwendet. In dieser Arbeit wird der erste Entwurf und Bau eines Mehrfrequenz-/Mehrzweck Pre-Prototyp Gyrotrons in koaxialer Technologie vorgestellt, das bei (136)/170/204 GHz mit einer Ausgangsleistung von 2 MW arbeitet. Dies ist der erste Schritt zum Betrieb bei Frequenzen bis zu 240 GHz unter Verwendung der Koaxialhohlraum-Gyrotrontechnologie. - A gyrotron is used in magnetically confined plasma experiments for heating, current drive, plasma stabilization and plasma diagnostics. This work presents the first design and construction of a multi-frequency / multi-purpose coaxial-cavity pre-prototype gyrotron operating at (136)/170/204 GHz with an output power of 2 MW. It is the first step towards operating frequencies up to 240 GHz using the coaxial-cavity gyrotron technology.
The DEMOnstration fusion power plant (DEMO) will be the first fusion reactor, which is intended to generate net electrical power. For successful operation of DEMO, high-power gyrotrons with operating frequencies up to 240 GHz are required for plasma heating and stabilization. In this work, a systematic feasibility study and tolerance analysis are performed for the conventional-type hollow-cavity DEMO gyrotrons. The various approaches are also suggested to identify its operational limits.
Magnetic confinement fusion relies on plasma heating and plasma control using gyrotron oscillators providing at megawatt power levels. The operational reliability decreases when operating at the performance limits due to increasing parasitic mode activity. This work demonstrates for the first time the automated, fast recovery of nominal gyrotron operation during a pulse by exploiting the hysteretic gyrotron behaviour after a mode switch being in use at the Wendelstein 7-X ECRH facility.
The physical design of cavity and magnetron injection gun (MIG) for a realistic, DEMO-compatible, coaxial-cavity 238 GHz 2 MW CW fusion gyrotron is developed in this work, having auxiliary frequencies at 170 GHz and 204 GHz. Novel systematic approaches towards multi-frequency mode selection, magnet requirements, and MIG design are presented. Mode deterioration and voltage depression variation due to insert misalignment versus cavity wall and/or versus electron beam are studied.