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This three-volume handbook provides an overview of the key aspects of micro process engineering. Volume 1 covers the fundamentals, operations and catalysts, volume 2 examines devices, reactions and applications, with volume 3 rounding off the trilogy with system, process and plant engineering. Fluid dynamics, mixing, heat/mass transfer, purification and separation microstructured devices and microstructured reactors are explained in the first volume. Volume 2 segments microreactor design, fabrication and assembly, bulk and fine chemistry, polymerisation, fuel processing and functional materials into understandable parts. The final volume of the handbook addresses microreactor systems design and scale-up, sensing, analysis and control, chemical process engineering, economic and eco-efficiency analyses as well as microreactor plant case studies in one book. Together, this 3-volume handbook explains the science behind micro process engineering to the scale-up and their real life industrial applications.
The last two decades have witnessed a rapid development of microelectromechanical systems (MEMS) involving gas microflows in various technical fields. Gas microflows can, for example, be observed in microheat exchangers designed for chemical applications or for cooling of electronic components, in fluidic microactuators developed for active flow control purposes, in micronozzles used for the micropropulsion of nano and picosats, in microgas chromatographs, analyzers or separators, in vacuum generators and in Knudsen micropumps, as well as in some organs-on-a-chip, such as artificial lungs. These flows are rarefied due to the small MEMS dimensions, and the rarefaction can be increased by low-...
With well over 90% of all processes in the industrial chemical production being of catalytic nature, catalysis is a mature though ever interesting topic. The idea of this book is to tackle various aspects of heterogeneous catalysis from the engineering point of view and go all the way from engineering of catalysis, catalyst preparation, characterization, reaction kinetics, mass transfer to catalytic reactors and the implementation of catalysts in chemical technology. Aimed for graduate students it is also a useful resource for professionals coming from the more academic side.
The widespread adoption of microreactors has been hindered by a lack of knowledge regarding rules and parameters needed for their design. This dissertation deals with the investigation of interfacial area and liquid mass transport in microreactors for gas/liquid reactions. Observations of a reduction in conversion occurring when changing from a glass laboratory device to a stainless steel process device motivated investigations into the effect of material and surface properties on the gas/liquid flow and reaction. This work takes a look inside the machined microstructures produced at the Institute for Micro Process Engineering of the Karlsruhe Institute of Technology and investigates the nat...
This work offers three solutions tailored to specific applications to overcome NMR challenges in the micro-domain. As the first sub-topic of this work, different potential electrode designs, compatible with NMR technique, are suggested and experimentally evaluated. As the second focus point, this work tackles multinuclear detection challenges. In parallel, a low-cost, broadband insert is discussed to enhance the sensitivity of standard NMR coils when a small sample volume is available.
This Special Issue compiles 11 scientific works that were presented during the International Symposium on Thermal Effects in Gas Flow in Microscale, ISTEGIM 2019, held in Ettlingen, Germany, in October 2019. This symposium was organized in the framework of the MIGRATE Network, an H2020 Marie Skłodowska-Curie European Training Network that ran from November 2015 to October 2019 (www.migrate2015.eu). MIGRATE intends to address some of the current challenges in innovation that face the European industry with regard to heat and mass transfer in gas-based microscale processes. The papers collected in this book focus on fundamental issues that are encountered in microfluidic systems involving gas...
This Special Issue compiles 11 scientific works that were presented during the International Symposium on Thermal Effects in Gas Flow in Microscale, ISTEGIM 2019, held in Ettlingen, Germany, in October 2019. This symposium was organized in the framework of the MIGRATE Network, an H2020 Marie Skłodowska-Curie European Training Network that ran from November 2015 to October 2019 (www.migrate2015.eu). MIGRATE intends to address some of the current challenges in innovation that face the European industry with regard to heat and mass transfer in gas-based microscale processes. The papers collected in this book focus on fundamental issues that are encountered in microfluidic systems involving gas...